You need:
- 200 flies
- mortar and pistle
- liquid nitrogen
- centrifugation vials (15 ml)
- 10 ml Dounce homogeniser with pestle
- Homogenisation buffer (10 mM Tris/HCl [pH7,5],
60 mM NaCl, 10 mM EDTA)
- Proteinase K (10 mg/ml)
- 10% SDS
- 3 M NaCl
- phenol-chloroform-IAA (50:49:1)
- chlorophorm-IAA (24:1).
- glass rods (made from 50µl glass capillaries)
- ethanol, ethanol (80%)
- microfuge, horizontal shaker
- Anesthesise flies (about 200) on ice, transfer them to a mortar
with liquid nitrogen (do not let the flies wake up and fly away) and grind
with a pistle until you get a homogenous powder of flies. Transfer the powder
to a cooled Dounce homogeniser containing 5 ml of homogenisation buffer
- Grind with a few strokes of the pestle to release cells and
nuclei from the caracasses of the flies. Centrifuge to remove debris at 1000
rpm for 1 min (but no more!).
- Transfer the supernatant with a pipette to a centrifugation tube,
spin in the Sorvall at 8000 rpm for 5 min.
- Discard the supernatant (cytoplasm with RNA), collect the pellet
(nuclei) and resuspend in 0,5 ml homogenisation buffer, transfer to a 2 ml
reaction vial.
- Add proteinase K to a final concentration of 100 µg/ml and
mix. Add 50 µl of 10% SDS and mix by swirling and rocking.
- incubate at 37°C for 45 to 60 min.
- Add 0.5 ml phenol/chloroform (wearing gloves!) and place tube
on a horizontal shaker for 5 min. (don't vortex - it would share large genomic
DNA to pieces; make sure the Eppendorf tube is firmly sealed with parafilm)
- Spin 3 min in microfuge at full speed, and transfer supernatant
into a new Eppendorf tube, use the P1000 pipetman; if the DNA is "gluey",
use a blue tip with a wider opening).
- Repeat step 5&6 with phenol-chloroform-IAA (50:49:1)
- Repeat step 5&6 with chlorophorm-IAA (24:1).
- Fill one Eppendorf tube with 1.5 ml 80% ethanol, another one
with 100% ethanol (for wash steps in 12.).
- Add NaCl to a final concentration of 200 mM, mix. Add two volumes
of 100% ethanol. Mix by gentle swirling. The DNA should appear at the interface
as a clump. After a white thread-like precipitate formed, use a Pasteur pipette
(glass hook) to transfer the precipitate to the tube with 80 % ethanol.
- Wash the precipitate in 80% ethanol and then 100% ethanol.
- Air-dry the precipitate to remove all ethanol and dislodge pellet
into 500 µl TE buffer.
- Rotate the tube on a horizontal shaker to dissolve the DNA.
- Take the OD260 from a 5 µl sample. A typical preparation yields
100-500 µg DNA. Store DNA at 4°C and clearly mark the number on
the tube.
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